2,6-Dichloroaniline → HCID 178514475, 화합물

HRID 626729노트

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HRID 626729 반응식
[N:1]([C:4]1[C:9](Cl)=[CH:8][N:7]=[CH:6][C:5]=1/[CH:11]=[N:12]/[C:13]1[C:20]([Cl:21])=[CH:19][C:16](C#N)=[CH:15][C:14]=1[Cl:22])=[N+:2]=[N-:3].N(C1C([Br:32])=CN=CC=1C=O)=[N+]=[N-].ClC1C=CC=C(Cl)C=1N>>[N:1]([C:4]1[C:9]([Br:32])=[CH:8][N:7]=[CH:6][C:5]=1/[CH:11]=[N:12]/[C:13]1[C:20]([Cl:21])=[CH:19][CH:16]=[CH:15][C:14]=1[Cl:22])=[N+:2]=[N-:3]

참가 물질

4

반응물 3

HCID 118462,6-DichloroanilineHCID 866970574-Azido-5-bromo-pyridine-3-carbaldehydeHCID 178509964HCID 178509964, 화합물

생성물 1

HCID 178514475HCID 178514475, 화합물

실험 절차

Following the procedure described for 4-{[1-(4-azido-5-chloropyridin-3-yl)meth-(E)-ylidene]amino}-3,5-dichlorobenzonitrile, 4-azido-5-bromopyridine-3-carbaldehyde and 2,6-dichloroaniline were reacted to afford the title compound as a beige solid that was used without purification.

후처리

  1. customwere reacted

출처 및 근거

ORD 기록
ord-b68ad5fcfb9443e39aadcd6567c60fa9
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09309240B2

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