Thionyl Chloride → HCID 58107439, 화합물

HRID 628144

반응식

HRID 628144 반응식
[Cl:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[F:14])[C:8](O)=[O:9])(=[O:4])=[O:3].S(Cl)([Cl:17])=O>CN(C=O)C>[Cl:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[F:14])[C:8]([Cl:17])=[O:9])(=[O:4])=[O:3]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 39298913-(Chlorosulfonyl)-4-fluorobenzoic acid

생성물 1

HCID 58107439HCID 58107439, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide촉매

실험 절차

3-(Chlorosulfonyl)-4-fluorobenzoic acid (1, 2.50 g, 10.5 mmol), thionyl chloride (10 mL) and DMF (1 drop) were heated at 90° C. for 1 hour and then the mixture evaporated to dryness. The material was used directly in the next step.

후처리

  1. customthe mixture evaporated to dryness

출처 및 근거

ORD 기록
ord-0d81ebdcd29843118ce9e289125ed5c6
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09309283B2

연결된 노트

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