돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 62838생성일: 2026년 10월 23일

3-(4-Hydroxyphenyl)propionic acid → Benzenepropanoic acid, 4-hydroxy-, methyl ester

https://huagongshe.com/ko/reaction/62838

반응식

참여 물질

역할이름HCID투입량
반응물3-(4-Hydroxyphenyl)propionic acidHCID 10394—
반응물1,4-Dioxane hydrochlorideHCID 20443148—
용매MethanolHCID 887—
생성물Benzenepropanoic acid, 4-hydroxy-, methyl esterHCID 79706100.5%

반응 단계

After 3-(4-hydroxy-phenyl)propionic acid (3 g, 18 mmol) was added with MeOH (6 mL), 4M HCl/dioxane solution (18 mL, 72 mmol) was added thereto, and the mixture was stirred at room temperature for 3 hours. The reactant was concentrated, added with EtOAc, and then washed with NaCl aqueous solution. The organic layer was separated, dried with MgSO4, and filtered to obtain the title compound (3.26 g, 99%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09447044B2
출처 데이터셋uspto-grants-2016_09
ORD IDord-ec3f833bd73143d4a3ef43c7709226b4
출처 메모uspto-grants-2016_09