3-Bromo-1,1,1-trifluoropropane → HCID 62033693, 화합물

HRID 62870

반응식

HRID 62870 반응식
[SH:1][C:2]1[N:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].Br[CH2:12][CH2:13][C:14]([F:17])([F:16])[F:15]>>[F:15][C:14]([F:17])([F:16])[CH2:13][CH2:12][S:1][C:2]1[N:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5]

참가 물질

3

반응물 2

HCID 27251143-Bromo-1,1,1-trifluoropropaneHCID 178524460HCID 178524460, 화합물

생성물 1

HCID 62033693HCID 62033693, 화합물수율 10%

실험 절차

2-Mercapto-nicotinic acid (1 g, 6.4 mmol) and 3-bromo-1,1,1-trifluoropropane were reacted in the same manner as in Step A of Preparation Example 10 to obtain the title compound (0.16 g, 10%).

출처 및 근거

ORD 기록
ord-1c1801a6c51a4b27bf71e7c919c5b737
출처 데이터셋
uspto-grants-2016_09
특허 번호
US09447044B2

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