Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Hydroxybenzaldehyde → 4-(3-Methylbutoxy)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Hydroxybenzaldehyde | HCID 126 | — |
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | 1-Iodo-3-methylbutane | HCID 10924 | — |
| 생성물 | 4-(3-Methylbutoxy)benzaldehyde | HCID 250101 | 92.6% |
반응 단계
The compound was synthesized as in Example 24.1, using 4-hydroxybenzaldehyde (200 mg, 1.64 mmol) and 1-iodo-3-methylbutane (649 mg, 1.97 mmol) in place of 1-chloro-3,3-dimethylbutane (no sodium iodide was used) to give 4-(isopentyloxy)benzaldehyde (292 mg, quant. crude) as a dark yellow oil that was used without further purification or characterization.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09315495B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-11006f97bdad4ecd9c18c5ee4f5e5d47 |
| 출처 메모 | uspto-grants-2016_04 |