4-Nitro-5-acetylaminoindazole → HCID 68264655, 화합물

HRID 629685

반응식

HRID 629685 반응식
[N+:1]([C:4]1[C:12]([NH:13]C(=O)C)=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[N:7][NH:8]2)([O-:3])=[O:2]>OS(O)(=O)=O>[N+:1]([C:4]1[C:12]([NH2:13])=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[N:7][NH:8]2)([O-:3])=[O:2]

참가 물질

3

반응물 1

HCID 682642654-Nitro-5-acetylaminoindazole

생성물 1

HCID 68264655HCID 68264655, 화합물수율 73.6%

시약·촉매·용매 1

HCID 1118Sulfuric Acid용매

실험 절차

By referring to the Step 5 of Example 1, 4-nitro-5-acetylaminoindazole (6.9 g, 31.5 mmol), 2 mol/L H2SO4 solution (200 mL), were used to obtain a product (4.0 g, 73.6%).

출처 및 근거

ORD 기록
ord-45e94c044202452ebbef01c251e5b09b
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09315513B2

연결된 노트

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