Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formaldehyde → (3-chloro-2H-indazol-2-yl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 3-Chloro-1H-indazole | HCID 95894 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | (3-chloro-2H-indazol-2-yl)methanol | HCID 59589510 | 99.7% |
반응 단계
In a 250 mL round bottom flask, 3-chloro-2H-indazole (1.95 g, 10 mmol), 30% HCHO (2 mL, 20 mmol) were mixed in water (10 mL). The reaction mixture was refluxed for 2 hours. After cooling down to room temperature, the solid was filtered, washed with water, and dried under vacuum to provide (3-chloro-2H-indazol-2-yl)methanol (1.82 g, 99% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09315521B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-df448b7d99c644bc9ce7349e01de42a3 |
| 출처 메모 | uspto-grants-2016_04 |