Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Fluoropyridine-4-carboxylic acid → HCID 77106318, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Fluoropyridine-4-carboxylic acid | HCID 345361 | — |
| 반응물 | 5-Methyl-2-furylmethylamine | HCID 2724683 | — |
| 생성물 | HCID 77106318 | HCID 77106318 | 34% |
반응 단계
The title compound was prepared in 34% yield from 5-methylfurfurylamine and 3-fluoroisonicotinic acid according to the procedure for the preparation of Example 3. 1H NMR (400 MHz, DMSO-d6): δ 13.45 (br s, 1H), 8.35 (s, 1H), 7.86 (d, 1H, J=5.0 Hz), 7.77 (br s, 1H), 7.57 (d, 1H, J=5.0 Hz), 6.24 (d, 1H, J=2.9 Hz), 6.00 (d, 1H, J=2.0 Hz), 4.50 (s, 2H), 2.23 (s, 3H). [M+H] calc'd for C12H12N2O3, 233. found 233.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447045B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-f70c0c2577eb4b678c5ffdf95e2f770f |
| 출처 메모 | uspto-grants-2016_09 |