Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Ethoxyphenol → HCID 23048282, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Ethoxyphenol | HCID 12150 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | HCID 23048282 | HCID 23048282 | — |
반응 단계
To a solution of 4-(ethyloxy)phenol (Commercial eg Aldrich) (1.0 g) in chloroform (5 ml) cooled to 0° C. was added bromine (1.26 g) dropwise over 20 min. The resulting mixture was stirred at 25 C. for 2 h, before washing sequentially with aqueous sodium bicarbonate, and brine. The organics were dried over sodium sulphate, filtered and concentrated in vacuo to yield the title compound, 1.8 g
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447074B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-b2f2eff8966742a39008bcd641da3c42 |
| 출처 메모 | uspto-grants-2016_09 |