Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyl bromide → HCID 178418677, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyl bromide | HCID 8002 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | HCID 178418594 | HCID 178418594 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178418677 | HCID 178418677 | — |
반응 단계
0.1 mol of 2,3-difluoro-4-(trans-4-pentylcyclohexyl)methoxyphenol, 0.11 mol of butyl bromide and 0.11 mol of potassium carbonate are heated for 16 hours at 100° in 100 ml of dimethylformamide (DMF). After cooling, the inorganic salts are filtered off with suction, the filtrate is concentrated, and water is added. 1-butyloxy-2,3-difluoro-4-(trans-4-pentylcyclohexyl)methoxybenzene is obtained by extraction with dichloromethane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05248447 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-709fc48404a84ef09737b5887db2472e |
| 출처 메모 | uspto-grants-1993_09 |