Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 2-Bromo-1-(6-methylpyridin-3-yl)ethanone hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 3-Acetyl-6-methylpyridine | HCID 95292 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-Bromo-1-(6-methylpyridin-3-yl)ethanone hydrobromide | HCID 45480511 | — |
반응 단계
500 mg (3.59 mmol) of 1-(6-methylpyrid-3-yl)ethanone, 590 μl (3.59 mmol) of hydrobromic acid, 204 μl (3.95 mmol) of bromine and 10 mL of glacial acetic acid were used in the reaction. After precipitation with ethyl ether and filtration, 1.02 g of 2-bromo-1-(6-methylpyrid-3-yl)ethanone hydrobromide are obtained, the characteristics of which are as follows:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09321790B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-eee58b6607064dc58e5a858551127640 |
| 출처 메모 | uspto-grants-2016_04 |