Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-4-methoxyaniline → N-(4-Methoxy-2-methylphenyl)-acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-4-methoxyaniline | HCID 7610 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 용매 | Dimethylacetamide | HCID 31374 | — |
| 생성물 | N-(4-Methoxy-2-methylphenyl)-acetamide | HCID 95082 | 88% |
반응 단계
Acetic anhydride (50 ml) was added dropwise to a solution of 4-methoxy-2-methylaniline (49.7 g, 360mmol) in DMA (200 ml) at 5° C. and the mixture stirred for 4.5 hours at ambient temperature. The solvent was removed by evaporation and the resulting solid washed with water and dried under vacuum to give N-(4-methoxy-2-methylphenyl)acetamide (57.3 g, 88%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06184225B2 |
| 출처 데이터셋 | uspto-grants-2001_02 |
| ORD ID | ord-176f1a6305aa4a55a6e8c9853f2cfc64 |
| 출처 메모 | uspto-grants-2001_02 |