Homophenylalanine, DL- → 2-Amino-4-phenylbutan-1-ol

HRID 634774

반응식

HRID 634774 반응식
[NH2:1][CH:2]([C:11](O)=[O:12])[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[NH2:1][CH:2]([CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH2:11][OH:12]

참가 물질

3

반응물 2

HCID 102530Homophenylalanine, DL-HCID 21226445Aluminium lithium hydride

생성물 1

HCID 131450362-Amino-4-phenylbutan-1-ol수율 78.1%

실험 절차

Following the general procedure of example 40b, DL-homophenylalanine (5.0 g, 27.9 mmol) was reduced with LiAlH4 to give (RS)-2-amino-4-phenyl-butan-1-ol (3.6 g, 78%, MS: m/e=166 (M+H+)) as a light yellow solid.

출처 및 근거

ORD 기록
ord-922d82ec72894955b59b642a49546f4e
출처 데이터셋
uspto-grants-2001_02
특허 번호
US06184236B2

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