Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → HCID 86756428, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | o-Toluenesulfonyl chloride | HCID 8623 | — |
| 반응물 | Benzaldehyde, 3-amino- | HCID 74366 | — |
| 반응물 | m-Toluenesulphonamide | HCID 74697 | — |
| 반응물 | HCID 21256445 | HCID 21256445 | — |
| 생성물 | HCID 86756428 | HCID 86756428 | — |
반응 단계
1-(2,3-Dimethylimidazo[2,1-b]-thiazol-5-yl ethanone (Formula N′-1), 0.97 g, was condensed with the 3-toluensulfonamide of benzaldehyde, m.p. 126-127°, prepared from toluene sulfonyl chloride and 3-aminobenzaldehyde, according to non-critical modifications of PREPARATION 15 to provide pure (E)-N-[3-[3-(2,3-Dimethylimidazo[2,1-b]thiazol-5-yl)-3-oxo-1-propenyl]phenyl-4-methylbenzenesulfonamide, m.p. 236-237°, Formula N′-2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06191124B1 |
| 출처 데이터셋 | uspto-grants-2001_02 |
| ORD ID | ord-ed899c7d24cd4a589abc1bab3ad8f41e |
| 출처 메모 | uspto-grants-2001_02 |