참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 반응물 | 2,2-Dimethyl-chroman-4-one | HCID 7454290 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2,2-Dimethyl-4-chromanone oxime | HCID 131722393 | — |
반응 단계
A reaction mixture prepared from 10 mmol of 2,2-dimethyl-4-chromanone, 12 mmol of hydroxylamine hydrochloride in 5 ml of methanol and 5 ml of pyridine is heated with stirring over the course of 2 hours to 80-85° C., the solvent is distilled off on a rotary evaporator and the oily residue is crystallized under water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06191164B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_02 |
|---|
| ORD ID | ord-8b926752e5bb4b5da7a24ab2bf4e3a79 |
|---|
| 출처 메모 | uspto-grants-2001_02 |
|---|
