Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl propiolate → HCID 178515908, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl propiolate | HCID 13536 | — |
| 반응물 | 3-Aminocyclohex-2-en-1-one | HCID 78892 | — |
| 생성물 | HCID 178515908 | HCID 178515908 | 21.3% |
반응 단계
A mixture of 3-amino-2-cyclohexen-1-one (25.0 g, 224.9 mmol) and methyl propiolate (23.6 g, 281 mmol) was heated to reflux for 1 h. The mixture was cooled and the solid was collected by filtration, washing with THF, to give 7.8 g (21%) of the title compound as a yellow solid. [M+H] calc'd for C9H9NO2, 164. found 164.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447046B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-3f3767687e84472091071ae2d9152061 |
| 출처 메모 | uspto-grants-2016_09 |