참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,5-Dinitrophenol | HCID 9492 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-Butene, 1,4-dibromo- | HCID 13180 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | 1-Bromo-4-(2,5-dinitrophenyloxy)but-2-ene | HCID 73994035 | — |
반응 단계
A mixture of 2,5-dinitrophenol (4.0 g), potassium carbonate (4.6 g), NMP (40 mL) and 1,4-dibromo-2-butene (14.0 g) is heated to 45° C. for 2 hr. Extraction in the normal fashion and Kugelrohr distillation of the excess dibromide (0.1 mm Hg, 800 C.) gives 1-bromo-4-(2,5-dinitrophenyloxy)but-2-ene (mp 81-83° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06194039B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_02 |
|---|
| ORD ID | ord-ac89a902efca444dac1a78793dc52b90 |
|---|
| 출처 메모 | uspto-grants-2001_02 |
|---|
