Dimethylamine → HCID 21254969, 화합물

HRID 636400노트

반응식

HRID 636400 반응식
Cl[C:2]1[N:7]2[N:8]=[C:9]([S:21][CH3:22])[C:10]([S:11]([C:14]3[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=3)(=[O:13])=[O:12])=[C:6]2[N:5]=[C:4]([CH3:23])[CH:3]=1.[CH3:24][NH:25][CH3:26]>CCO>[Cl:20][C:17]1[CH:18]=[CH:19][C:14]([S:11]([C:10]2[C:9]([S:21][CH3:22])=[N:8][N:7]3[C:2]([N:25]([CH3:26])[CH3:24])=[CH:3][C:4]([CH3:23])=[N:5][C:6]=23)(=[O:12])=[O:13])=[CH:15][CH:16]=1

참가 물질

4

반응물 2

HCID 674DimethylamineHCID 212549867-Chloro-3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidine

생성물 1

HCID 21254969HCID 21254969, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

In an analogous manner to that described in Example 5, from 7-chloro-3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidine and dimethyl-amine in EtOH there was obtained [3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidin-7-yl]-dimethyl-amine as colorless crystals, m.p. 221-223°.

출처 및 근거

ORD 기록
ord-96f129ed65e14d3aa4e889ef5232ddbb
출처 데이터셋
uspto-grants-2001_02
특허 번호
US06194410B1

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