Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → HCID 118597990, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | 1,3-Dihydro-2-benzofuran-5-amine | HCID 12445339 | — |
| 생성물 | HCID 118597990 | HCID 118597990 | 69% |
반응 단계
1,3-Dihydro-2-benzofuran-5-amine (300 mg, 2.2 mmol) was added to HCOOH (10 mL), and the reaction was stirred at reflux overnight. The reaction was concentrated, basified to pH=8 with sat Na2CO3, and extracted with EtOAc. Organics were washed with brine, dried (Na2SO4), and concentrated to give 250 mg (69%) of N-(1,3-dihydro-2-benzofuran-5-yl)formamide as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447046B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-7535fa64e1b44f0aa936eef954ce8d4b |
| 출처 메모 | uspto-grants-2016_09 |