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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 63643생성일: 2026년 10월 25일

Formic Acid → HCID 118597990, 화합물

https://huagongshe.com/reaction/63643

반응식

참여 물질

역할이름HCID투입량
반응물Formic AcidHCID 284—
반응물1,3-Dihydro-2-benzofuran-5-amineHCID 12445339—
생성물HCID 118597990HCID 11859799069%

반응 단계

1,3-Dihydro-2-benzofuran-5-amine (300 mg, 2.2 mmol) was added to HCOOH (10 mL), and the reaction was stirred at reflux overnight. The reaction was concentrated, basified to pH=8 with sat Na2CO3, and extracted with EtOAc. Organics were washed with brine, dried (Na2SO4), and concentrated to give 250 mg (69%) of N-(1,3-dihydro-2-benzofuran-5-yl)formamide as a yellow oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09447046B2
출처 데이터셋uspto-grants-2016_09
ORD IDord-7535fa64e1b44f0aa936eef954ce8d4b
출처 메모uspto-grants-2016_09