Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Ethyl 2-(2-formyl-6-methoxyphenoxy)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ethyl bromoacetate | HCID 7748 | — |
| 반응물 | o-Vanillin | HCID 8991 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Ethyl 2-(2-formyl-6-methoxyphenoxy)acetate | HCID 2229635 | — |
반응 단계
A solution of 2-hydroxy-3-methoxybenzaldehyde (6.08 g), ethyl bromoacetate (4.9 ml) and potassium carbonate (12.14 g) in N,N-dimethylformamide (30 ml) was stirred for 2 hours at ambient temperature. Water was added to the reaction mixture, and the resulting precipitates were collected by filtration and recrystallized with ethanol to give 2-ethoxycarbonylmethoxy-3-methoxybenzaldehyde (5.04 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06194396B1 |
| 출처 데이터셋 | uspto-grants-2001_02 |
| ORD ID | ord-abc85a8fd79b40dfa5f86e47ceefd32a |
| 출처 메모 | uspto-grants-2001_02 |