Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dabco → Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dabco | HCID 9237 | — |
| 반응물 | 2,2'-Oxybisethanethiol | HCID 75073 | — |
| 반응물 | 1,4-Butanedisulfonyl dichloride | HCID 315317 | — |
| 생성물 | Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chloride | HCID 86756468 | — |
반응 단계
The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06194487B1 |
| 출처 데이터셋 | uspto-grants-2001_02 |
| ORD ID | ord-c8607af1eb714855bbe19d2842843eca |
| 출처 메모 | uspto-grants-2001_02 |