참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | — |
| 반응물 | Dimethyl sulphoximine potassium salt | HCID 86740516 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine | HCID 20256530 | — |
반응 단계
A solution of 99.3 g of m-acetoxybenzoyl chloride in 150 ml of absolute tetrahydrofuran is added dropwise at -35° C. during 20 minutes while stirring to the dimethyl sulphoximine potassium salt suspension and the mixture is then stirred at -35° C. for 30 minutes. N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine is thus formed in suspension.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04556413 |
|---|
| 출처 데이터셋 | uspto-grants-1985_12 |
|---|
| ORD ID | ord-7abe3c7ad9e0455ab3840a266774c0b4 |
|---|
| 출처 메모 | uspto-grants-1985_12 |
|---|
