Dimethylformamide → HCID 13362252, 화합물

HRID 637331

반응식

HRID 637331 반응식
S([C:5]1[CH:11]=[CH:10][C:8](C)=[CH:7][CH:6]=1)([O-])(=O)=O.[O-:12][C:13]1C=CC=[CH:15][CH:14]=1.[K+].[CH3:20][N:21]([CH3:24])[CH:22]=[O:23]>>[CH3:20][N:21]1[CH2:24][CH:14]([CH2:13][O:12][C:5]2[CH:6]=[CH:7][CH:8]=[CH:10][CH:11]=2)[CH2:15][C:22]1=[O:23]

참가 물질

4

반응물 3

HCID 6228DimethylformamideHCID 85570p-ToluenesulfonateHCID 23670670Potassium phenoxide

생성물 1

HCID 13362252HCID 13362252, 화합물

실험 절차

A solution of the resulting tosylate (21.5 g; 0.075 mole) and of potassium phenoxide (10 g; 0.075 mole) in dimethylformamide (150 ml) is refluxed for 2 hrs.

출처 및 근거

ORD 기록
ord-d84526e153214697b4cb8e1d5ae29157
출처 데이터셋
uspto-grants-1985_12
특허 번호
US04556674

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