N-[(Phenylmethoxy)carbonyl]-L-isoleucine → HCID 54257317, 화합물

HRID 637640

반응식

HRID 637640 반응식
[C:1]([NH:11][C@H:12]([C:17]([OH:19])=O)[C@H:13]([CH2:15][CH3:16])[CH3:14])([O:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:2].[N:20]1[CH:25]=[CH:24][CH:23]=[C:22]([NH:26][CH2:27][C:28]([O:30][CH2:31][CH3:32])=[O:29])[CH:21]=1>C(Cl)Cl>[C:1]([NH:11][C@H:12]([C:17]([N:26]([C:22]1[CH:21]=[N:20][CH:25]=[CH:24][CH:23]=1)[CH2:27][C:28]([O:30][CH2:31][CH3:32])=[O:29])=[O:19])[C@H:13]([CH2:15][CH3:16])[CH3:14])([O:3][CH2:4][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=1)=[O:2]

참가 물질

4

반응물 2

HCID 2724772N-[(Phenylmethoxy)carbonyl]-L-isoleucineHCID 20255549ethyl N-(3-pyridyl)-glycinate

생성물 1

HCID 54257317HCID 54257317, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

A methylene chloride solution of N-carbobenzyloxy-L-isoleucine and ethyl N-(3-pyridyl)-glycinate was treated with N,N-dicyclohexylcarbodiimide as in example 5A. Purification of the product was accomplished by chromatography on silica-gel.

후처리

  1. customPurification of the product

출처 및 근거

ORD 기록
ord-a1fdac81623e4d5791d08979bc3bd5fa
출처 데이터셋
uspto-grants-1985_12
특허 번호
US04558038

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