Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → 5-Thiazolecarboxamide, N,4-dimethyl-2-(4-methoxyphenyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Ethyl 2-(4-methoxyphenyl)-4-methyl-1,3-thiazole-5-carboxylate | HCID 7540952 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-Thiazolecarboxamide, N,4-dimethyl-2-(4-methoxyphenyl)- | HCID 3068076 | 69% |
반응 단계
Into a mixed solvent of 80 ml of 40% methylamine and 600 ml of ethanol, 13.9 g of ethyl 2-(4-methoxyphenyl)-4-methylthiazole-5-carboxylate was dissolved. Then, in a similar manner as in Example 1, the object was obtained as colourless minute aciculate melting at 157.5° to 159° C. in an amount of 9.1 g corresponding to the yield of 69%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04558059 |
| 출처 데이터셋 | uspto-grants-1985_12 |
| ORD ID | ord-32fcbd1c17634c8d955f3fb3536b1d48 |
| 출처 메모 | uspto-grants-1985_12 |