참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfamic Acid | HCID 5987 | — |
| 반응물 | Dicyandiamide | HCID 10005 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178513042 | HCID 178513042 | 181.9% |
반응 단계
Dicyandiamide (84 g) was suspended in 80 ml of water and reacted successively with 97 g sulfaminic acid at 80° C. in such manner that the temperature of 95° C. was not exceeded. The reaction mixture was agitated for another 15 minutes at 95° C. Then the solution was rapidly cooled to 0° C.-5° C., and the resultant colorless crystals were drawn off and washed with 100 ml ethanol. After drying, 181 g (91%) guanylurea sulfamate was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04559409 |
|---|
| 출처 데이터셋 | uspto-grants-1985_12 |
|---|
| ORD ID | ord-8527a224217847a2962967f7ec5bf61e |
|---|
| 출처 메모 | uspto-grants-1985_12 |
|---|
