Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[1,3]Oxathiolo[5,4-c]pyridin-6-ylmethanol → [1,3]Oxathiolo[5,4-c]pyridine-6-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [1,3]Oxathiolo[5,4-c]pyridin-6-ylmethanol | HCID 67426109 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | [1,3]Oxathiolo[5,4-c]pyridine-6-carbaldehyde | HCID 59254367 | 62.3% |
반응 단계
[1,3]oxathiolo[5,4-c]pyridine-6-methanol (0.92 g, 5.44 mmole) was treated with manganese (IV) oxide (3.83 g, 44 mmole) at RT in DCM (50 mL) to afford the aldehyde (567 mg, 62%) as a solid; MS (+ve ion electrospray) m/z 168 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07691850B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-e811c26613054254a23fc21a8c0d7428 |
| 출처 메모 | uspto-grants-2010_04 |