Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl Acrylate → HCID 15696577, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl Acrylate | HCID 8821 | — |
| 반응물 | Ethyl 3-aminobutyrate | HCID 98103 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 15696577 | HCID 15696577 | — |
반응 단계
A solution of ethyl 3-aminobutanoate (4.2 g) and of ethyl 2-propenoate (3.83 mL) in EtOH (20 mL) was stirred at room temperature for 8 h. The solvent was evaporated under reduced pressure and the residue purified by chromatography on NH column eluting with a gradient from 100% cyclohexane to 90% ethyl acetate/cyclohexane. The title compound was isolated as a colourless oil, 3.9 g (MS (m/z): 232 [MH]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07691893B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-266854fc87104b09ac26d16514c66928 |
| 출처 메모 | uspto-grants-2010_04 |