HCID 86617366, 화합물 → HCID 68428157, 화합물

HRID 642427노트

반응식

HRID 642427 반응식
[CH2:1]([O:3][C:4]([C:6]1[N:18]=[C:17](Br)[C:16]2[C:15]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[N:9]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8]=2[C:7]=1[OH:26])=[O:5])[CH3:2].[C:27]([Cu])#[N:28]>>[CH2:1]([O:3][C:4]([C:6]1[N:18]=[C:17]([C:27]#[N:28])[C:16]2[C:15]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[N:9]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8]=2[C:7]=1[OH:26])=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 86617366HCID 86617366, 화합물HCID 178418546HCID 178418546, 화합물

생성물 1

HCID 68428157HCID 68428157, 화합물

실험 절차

Prepared in analogy to that of Example 105(a) from 1-bromo-4-hydroxy-5-phenyl-5H-pyrido[4,3-b]indole-3-carboxylic acid ethyl ester and CuCN. The title compound, ESI MS (m/z): 358 (M+H)+.

출처 및 근거

ORD 기록
ord-f8f2284c94f043d6b18f8fd3c9d7204d
출처 데이터셋
uspto-grants-2010_04
특허 번호
US07696223B2

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