Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Cyclopenten-1-one → 6,6-Diethoxybicyclo[3.2.0]heptan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Cyclopenten-1-one | HCID 13588 | — |
| 반응물 | 1,1-Diethoxyethene | HCID 137673 | — |
| 용매 | Pentane | HCID 8003 | — |
| 생성물 | 6,6-Diethoxybicyclo[3.2.0]heptan-2-one | HCID 12564365 | — |
반응 단계
To a solution of cyclopent-2-enone (3.7 g, 45 mmol) in pentane (80 mL) was added 1,1-diethoxyethene (89 mL, 677 mmol). The mixture was put in an ACE Photo Reactor (450 W lamp), and stirred at RT for 20 hr. It was concentrated to give the title compound as a pale yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07696241B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-cb3b74a5e9a4424bb222409ea0cf03ea |
| 출처 메모 | uspto-grants-2010_04 |