2-(Acetyloxy)-5-chlorobenzoic acid → Benzamide,2-(acetyloxy)-5-chloro-n-1(2h)-pyridazinyl-

반응식

[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][C:6]=1[C:7]([OH:9])=O)(=[O:3])[CH3:2].[NH2:15][N:16]1[CH:21]=[CH:20][CH:19]=[CH:18][NH:17]1>>[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][C:6]=1[C:7]([NH:15][N:16]1[CH:21]=[CH:20][CH:19]=[CH:18][NH:17]1)=[O:9])(=[O:3])[CH3:2]

참가 물질

반응물 2

HCID 28208132-(Acetyloxy)-5-chlorobenzoic acid

HCID 222262352-Aminopyridazine

생성물 1

HCID 23069950Benzamide,2-(acetyloxy)-5-chloro-n-1(2h)-pyridazinyl-수율 19.7%

실험 절차

Using 2-acetoxy-5-chlorobenzoic acid and 2-aminopyridazine as the raw materials, the same operation as the Example 198(3) gave the title compound.

출처 및 근거

ORD 기록: ord-5d4f82d8b53d46649b3ce8b8c6aebb42
출처 데이터셋: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07700655B2

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