Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexanol → Cyclohexyloxy cyclopentyl dimethoxysilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexanol | HCID 7966 | — |
| 반응물 | Cyclopentyltrimethoxysilane | HCID 9855701 | — |
| 촉매 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | Cyclohexyloxy cyclopentyl dimethoxysilane | HCID 19793816 | 83.3% |
반응 단계
The procedures of Example 2 were repeated with the exception that 10.0 g (0.0526 mole) of cyclopentyl trimethoxysilane, 85.1 mg (1.58 m mole) of sodium methoxide, and 52.7 g (0.526 mole) of cyclohexanol in place of sec-butyl alcohol were used and the reaction time was one and a half hours. Then, 11.3 g (0.0438 mole) of cyclohexyloxy cyclopentyl dimethoxysilane were obtained. Its structure was confirmed as in Example 1. FIGS. 3 and 4 are the charts of 1H-NMR and IR, respectively. The yield was 83%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05248803 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-dfdccf328d594417823f1d891b869737 |
| 출처 메모 | uspto-grants-1993_09 |