Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | 2-[4-(2-Quinoxalinyloxy)phenoxy]propionyl chloride | HCID 13670532 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate | HCID 13670534 | — |
반응 단계
To a solution of 1.2 g allyl alcohol and 1.6 g pyridine in 50 cc methylene chloride, add 6.6 g of 2-[4-(2-quinoxalinyloxy)phenoxy]propionyl chloride in 60 cc methylene chloride. Stir the mixture at room temperature overnight. Wash the methylene chloride solution with water and dry the solution over magnesium sulfate concentrate under vacuum to give allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04609396 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-a9135ae31a7f4357adf017005813a8cd |
| 출처 메모 | uspto-grants-1986_09 |