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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 64602생성일: 2026년 10월 23일

Methyldichlorosilane → Silane, dichloro-5-hexen-1-ylmethyl-

https://huagongshe.com/ko/reaction/64602

반응식

참여 물질

역할이름HCID투입량
반응물MethyldichlorosilaneHCID 6376—
반응물1,5-HexadieneHCID 11598—
생성물Silane, dichloro-5-hexen-1-ylmethyl-HCID 1106337387.6%

반응 조건

온도40 °C

반응 단계

5-Hexenylmethyldichlorosilane was prepared by combining 1,5-hexadiene (160 g, 1.95 m), 0.1 g of a platinum complex ##STR1## and methyldichlorosilane (5 g) in a flask equipped with a condenser and a thermometer. The mixture was heated to 40° C. to initiate the reaction. Additional methyldichlorosilane (120 g) was added dropwise to the mixture so that the temperature was kept below 55° C. The product was isolated in 87.6% yield by distillation under reduced pressure (bp 67°-9° C./2 mm Hg).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04609574
출처 데이터셋uspto-grants-1986_09
ORD IDord-3130f4ffee2a4a87bfd4963f21ea6fd7
출처 메모uspto-grants-1986_09