참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methyldichlorosilane | HCID 6376 | — |
| 반응물 | 1,5-Hexadiene | HCID 11598 | — |
| 생성물 | Silane, dichloro-5-hexen-1-ylmethyl- | HCID 11063373 | 87.6% |
반응 단계
5-Hexenylmethyldichlorosilane was prepared by combining 1,5-hexadiene (160 g, 1.95 m), 0.1 g of a platinum complex ##STR1## and methyldichlorosilane (5 g) in a flask equipped with a condenser and a thermometer. The mixture was heated to 40° C. to initiate the reaction. Additional methyldichlorosilane (120 g) was added dropwise to the mixture so that the temperature was kept below 55° C. The product was isolated in 87.6% yield by distillation under reduced pressure (bp 67°-9° C./2 mm Hg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04609574 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
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| ORD ID | ord-3130f4ffee2a4a87bfd4963f21ea6fd7 |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|