참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3,5-Dimethylphenol | HCID 7948 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1,4-Dichlorobutanol | HCID 19347542 | — |
| 생성물 | 4-Chloro-1-(3,5-dimethylphenoxy)-2-butanol | HCID 13120344 | — |
반응 단계
To a mixture of 245 g. (2 moles) of 3,5-dimethylphenol and 2 liters of 2N sodium hydroxide was added 2.5 moles of 1,4-dichlorobutanol with stirring at 65° C. overnight. The solid precipitate which separated on cooling was filtered and washed with water to neutrality. Recrystallization with isopropyl ether yielded 375 g. of white crystalline solid which melted at 74°-76° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04609735 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
|---|
| ORD ID | ord-ac41ec0c18c44ca8a3fe37648a717c89 |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|
