Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4-Chloro-1-(4-chloro-2-methylphenoxy)-2-butanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 4-Chloro-2-methylphenol | HCID 14855 | — |
| 반응물 | 1,4-Dichloro-2-butanol | HCID 17021 | — |
| 용매 | tert-Butanol | HCID 6386 | — |
| 생성물 | 4-Chloro-1-(4-chloro-2-methylphenoxy)-2-butanol | HCID 13120346 | — |
반응 단계
4-Chloro-1-(4-chloro-2-methylphenoxy)-2-butanol was prepared according to the procedure of Preparation 4 using 105 g. (0.74 mole) of 2-methyl-4-chlorophenol, 171.5 g. (1.2 mole) of 1,4-dichloro-2-butanol, 50.3 g. of sodium hydroxide, 300 ml. of water and 300 ml. of tertiary butanol. There was obtained 84 g. (45.5%) of product which distilled at 135° C./0.01 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04609735 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-008d879749ca4fe7974966c270b01e5d |
| 출처 메모 | uspto-grants-1986_09 |