Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chlorophenol → 4-Chloro-1-(4-chlorophenoxy)-2-butanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chlorophenol | HCID 4684 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1,4-Dichloro-2-butanol | HCID 17021 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-Chloro-1-(4-chlorophenoxy)-2-butanol | HCID 13120349 | — |
반응 단계
4-Chloro-1-(4-chlorophenoxy)-2-butanol was prepared using the procedure of Preparation 7 from 45 g. (0.5 mole) of p-chlorophenol, 72 g. (0.5 mole) of 1,4-dichloro-2-butanol, 40 g. (1.0 mole) of sodium hydroxide and 400 ml. of water to give 85 g. (36.1%) of product which melted at 62°-64° C. after recrystallization from isopropanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04609735 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-b8932352aad64fcea11992d6264bd36e |
| 출처 메모 | uspto-grants-1986_09 |