Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → 7-nitro-1H-indene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 4-Nitro-2,3-dihydro-1H-inden-1-OL | HCID 13102456 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 7-nitro-1H-indene | HCID 13239587 | 44.5% |
반응 단계
In the manner of Example 1, step I, 14.0 g (0.078 mole) of 4-nitro-1-indanol (compound D, schema 1, prepared as in Example 1, step D) was heated in the presence of 0.1 g of p-toluenesulfonic acid and 200 mL of toluene to give 5.6 g of 7-nitro-1H-indene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04408057 |
| 출처 데이터셋 | uspto-grants-1983_10 |
| ORD ID | ord-74ecf79e1172425f824e46efb4815847 |
| 출처 메모 | uspto-grants-1983_10 |