Potassium Hydroxide → 4-(1-Pyrrolyl)-2-indanol

HRID 647318노트

반응식

HRID 647318 반응식
C([O:4][CH:5]1[CH2:13][C:12]2[C:7](=[CH:8][CH:9]=[CH:10][C:11]=2[N:14]2[CH:18]=[CH:17][CH:16]=[CH:15]2)[CH2:6]1)(=O)C.[OH-].[K+]>O.C(O)C>[N:14]1([C:11]2[CH:10]=[CH:9][CH:8]=[C:7]3[C:12]=2[CH2:13][CH:5]([OH:4])[CH2:6]3)[CH:15]=[CH:16][CH:17]=[CH:18]1

참가 물질

5

반응물 2

HCID 14797Potassium HydroxideHCID 132395854-(1-Pyrrolyl)-2-indanyl acetate

생성물 1

HCID 132395814-(1-Pyrrolyl)-2-indanol수율 52.7%

시약·촉매·용매 2

HCID 702Ethanol용매HCID 962Water용매

실험 절차

In the manner of Example 1, step H, hydrolysis of 0.84 g (0.004 mole) of 4-(1-pyrrolyl)-2-indanyl acetate with 0.28 g (0.005 mole) of potassium hydroxide in 5 mL of water and 10 mL of ethanol gave 0.42 g of 4-(1-pyrrolyl)-2-indanol.

출처 및 근거

ORD 기록
ord-25120d00e71d4fc390a83fdd78e88074
출처 데이터셋
uspto-grants-1983_10
특허 번호
US04408057

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