Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bis(2-chloroethyl) ether → 1,5-Bis(4-iodophenoxy)-3-oxapentane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bis(2-chloroethyl) ether | HCID 8115 | — |
| 반응물 | 4-Iodophenol | HCID 10894 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | 1,5-Bis(4-iodophenoxy)-3-oxapentane | HCID 19021957 | — |
반응 단계
A mixture prepared by adding 3.08 g of sodium hydroxide and 40 ml of n-butanol to 15.4 g of 4-iodophenol was refluxed. 2 ml of n-butanol solution of 5.01 g of 1,5-dichloro-3-oxapentane was added dropwise to the above prepared mixture over a period of 5 minutes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05248826 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-de601d7504a04544afaf93084d42b5be |
| 출처 메모 | uspto-grants-1993_09 |