HCID 178490397, 화합물 → BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)-

HRID 647603노트

반응식

HRID 647603 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:19]=[CH:20][CH:21]=1)[CH:6]=[N:7][NH:8][C:9]1[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[CH2:12][O:11][N:10]=1>C1(C)C(C)=CC=CC=1>[OH:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:9]1[NH:8][N:7]=[C:6]([C:5]2[CH:19]=[CH:20][CH:21]=[C:3]([O:2][CH3:1])[CH:4]=2)[N:10]=1

참가 물질

3

반응물 1

HCID 178490397HCID 178490397, 화합물

생성물 1

HCID 53228BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)-

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

A suspension of 16 g of 4-[2-(3-methoxybenzyliden)hydrazino]-1H-2,3-benzoxazine in 160 cc of anhydrous xylene is refluxed for 45 minutes and then, cooled in an ice bath. The solid which precipitates is recovered by filtration and recrystallized from ethanol yielding 14.7 g of the compound of the title. M.p. 157°-59° C.

후처리

  1. temperatureis refluxed for 45 minutes
  2. temperaturecooled in an ice bath
  3. customThe solid which precipitates
  4. filtrationis recovered by filtration
  5. customrecrystallized from ethanol yielding 14.7 g of the compound of the title

출처 및 근거

ORD 기록
ord-7d8462bd23b44b4ab9a60edb9bfd093f
출처 데이터셋
uspto-grants-1983_10
특허 번호
US04409388

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