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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 647796생성일: 2026년 10월 25일

Thionyl Chloride → Methyl 2-(dimethylamino)-N-[[[[[(diethoxyphosphinothioyl)isopropylamino]sulfinyl]methylamino]carbonyl]oxy]-2-oxoethanimidothioate

https://huagongshe.com/reaction/647796

반응식

참여 물질

역할이름HCID투입량
반응물Thionyl ChlorideHCID 24386—
반응물OxamylHCID 31657—
반응물Phosphoramidothioic acid, (1-methylethyl)-, O,O-diethyl esterHCID 778771—
용매PyridineHCID 1049—
생성물Methyl 2-(dimethylamino)-N-[[[[[(diethoxyphosphinothioyl)isopropylamino]sulfinyl]methylamino]carbonyl]oxy]-2-oxoethanimidothioateHCID 86739081—

반응 단계

Methyl 2-(dimethylamino)-N-[[[[[(diethoxyphosphinothioyl)isopropylamino]sulfinyl]methylamino]carbonyl]oxy]-2-oxoethanimidothioate was prepared by the procedure employed in Example 21, by reacting methyl 2-(dimethylamino)-N-[[(methylamino)carbonyl]oxy]-2-oxoethanimidothioate (3.29 g, 0.015 mole), thionyl chloride (1.79 g, 0.015 mole), and O,O-diethyl isopropylphosphoramidothioate (3.17 g, 0.015 mole) in pyridine (10 ml). Column chromatography afforded 2.6 g of an oil of the formula below, nD24 1.5211 ##STR42##

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04410518
출처 데이터셋uspto-grants-1983_10
ORD IDord-bc98f0a394bd4856a913cc31935e8b76
출처 메모uspto-grants-1983_10