Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl Peroxide → 4-(4-Methoxybenzoyl)benzyl bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | (4-Methoxyphenyl)(4-methylphenyl)methanone | HCID 32113 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 4-(4-Methoxybenzoyl)benzyl bromide | HCID 13150670 | 29.2% |
반응 단계
Benzoyl peroxide (1 g) was added to a solution of 4-methoxyphenyl-4-methylphenyl methanone (22.6 g) and N-bromosuccinimide (17.8 g) in CCl4 (100 ml). The mixture was heated under reflux for 3.25 h, then cooled to 0°. The precipitated succinimide was filtered off, the filtrate evaporated and the residue purified by crystallisation from cyclohexane to give the title compound (8.9 g), m.p. 76°-78°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04410521 |
| 출처 데이터셋 | uspto-grants-1983_10 |
| ORD ID | ord-0b787cae83ac48669327f043bb8ae569 |
| 출처 메모 | uspto-grants-1983_10 |