HCID 13092093, 화합물 → 5-(2-Formyl-3-hydroxyphenoxy)pentanoic acid

HRID 647899

반응식

HRID 647899 반응식
[CH:1]([C:3]1[C:16]([O:17]CC2C=CC=CC=2)=[CH:15][CH:14]=[CH:13][C:4]=1[O:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:2]>C(O)C>[CH:1]([C:3]1[C:16]([OH:17])=[CH:15][CH:14]=[CH:13][C:4]=1[O:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:2]

참가 물질

3

반응물 1

HCID 13092093HCID 13092093, 화합물

생성물 1

HCID 721625-(2-Formyl-3-hydroxyphenoxy)pentanoic acid

시약·촉매·용매 1

HCID 702Ethanol촉매

실험 절차

A solution of 5-(2-formyl-3-benzyloxyphenoxy) pentanoic acid (1.0 g, 0.003 M) in ethanol containing 5% palladium on charcoal catalyst (0.61 g) was hydrogenated at atmospheric pressure. After 20 minutes the reaction was complete and the catalyst was filtered off and the ethanol removed in vacuo to give 5-(2-formyl-3-hydroxyphenoxy)pentanoic acid, m.p. 94° C.

후처리

  1. filtrationthe catalyst was filtered off
  2. customthe ethanol removed in vacuo

출처 및 근거

ORD 기록
ord-9d0b78254b974d9ba476916954126963
출처 데이터셋
uspto-grants-1983_10
특허 번호
US04410537

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