1-Propyl-4-piperidone → 9-Propyl-7,8,9,10-tetrahydrothieno[3,2-e]pyrido[4,3-b]indole

반응식

Cl.[NH:2]([C:4]1[CH:5]=[CH:6][C:7]2[S:11][CH:10]=[CH:9][C:8]=2[CH:12]=1)N.[CH2:13]([N:16]1[CH2:21][CH2:20][C:19](=O)[CH2:18][CH2:17]1)[CH2:14][CH3:15]>>[CH2:13]([N:16]1[CH2:21][CH2:20][C:19]2[NH:2][C:4]3[C:12]([C:18]=2[CH2:17]1)=[C:8]1[CH:9]=[CH:10][S:11][C:7]1=[CH:6][CH:5]=3)[CH2:14][CH3:15]

참가 물질

반응물 2

HCID 900061-Propyl-4-piperidone

HCID 20484314(1-Benzothiophen-5-yl)hydrazine hydrochloride

생성물 1

HCID 204843039-Propyl-7,8,9,10-tetrahydrothieno[3,2-e]pyrido[4,3-b]indole

실험 절차

This compound is formed analogously to that described in Example 15, from 2 g of 5-hydrazinobenzothiophene hydrochloride and 1.7 g of 1-propyl-4-piperidone. Melting point: 143°-144° C.

후처리

customThis compound is formed analogously to that

출처 및 근거

ORD 기록: ord-075b6ca8677d4434803549b59ba4c6bd
출처 데이터셋: uspto-grants-1983_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04410536

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