p-Bromobenzenesulfonyl chloride → 4-Bromo-N-[2-(1H-imidazol-1-yl)ethyl]benzenesulfonamide
반응식
[N:1]1([CH2:6][CH2:7][NH2:8])[CH:5]=[CH:4][N:3]=[CH:2]1.[Br:9][C:10]1[CH:15]=[CH:14][C:13]([S:16](Cl)(=[O:18])=[O:17])=[CH:12][CH:11]=1>>[Br:9][C:10]1[CH:15]=[CH:14][C:13]([S:16]([NH:8][CH2:7][CH2:6][N:1]2[CH:5]=[CH:4][N:3]=[CH:2]2)(=[O:18])=[O:17])=[CH:12][CH:11]=1참가 물질
3
실험 절차
When 1H-imidazole-1-ethanamine was treated with 4-bromobenzenesulfonyl chloride by the procedure of Example 20, the compound of this example, mp 165°-167° C., was obtained.
출처 및 근거
- ORD 기록
- ord-b2d2a8b7c3874c64be8a0b528b437629
- 출처 데이터셋
- uspto-grants-1986_09
- 특허 번호
- US04610981
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