Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Anisoyl chloride → HCID 13371227, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Anisoyl chloride | HCID 7477 | — |
| 반응물 | 1-(Morpholinocarbonylmethyl)piperazine | HCID 100622 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 13371227 | HCID 13371227 | — |
반응 단계
10.25 g of piperazin-1-yl-acetic acid morpholide are cooled to 0° C. in 20 ml of methylene chloride. 8.75 g of anisoyl chloride are added dropwise in the course of 15 minutes. After the mixture has been subsequently stirred for 4 hours, it is diluted with isopropanol, whereupon the colourless product precipitates. It is filtered off with suction and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04610984 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-21ca3ae338254865a0d42275bcf052d1 |
| 출처 메모 | uspto-grants-1986_09 |