참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | p-Anisoyl chloride | HCID 7477 | — |
| 반응물 | 1-((Pyrrolidine-1-carbonyl)methyl)piperazine | HCID 100614 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-(4-Methoxybenzoyl)-piperazin-1-yl-acetic acid pyrrolidide hydrochloride | HCID 13371229 | — |
반응 단계
9.4 g of piperazin-1-yl-acetic acid pyrrolidide are dissolved in 10 ml of methylene chloride. A solution of 8.75 g of anisic acid chloride in 10 ml of methylene chloride is added dropwise at 0°. After the mixture had been stirred at 25° C. for 60 minutes, the crystals are filtered off with suction and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04610984 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
|---|
| ORD ID | ord-4b04545c2c6a4b479b8c744174660109 |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|
