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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 648912생성일: 2026년 10월 25일

1-Methylpiperazine → Piperazinium, 1-(1,3-dithiol-2-ylidene)-4-methyl-, perchlorate

https://huagongshe.com/reaction/648912

반응식

참여 물질

역할이름HCID투입량
반응물1-MethylpiperazineHCID 53167—
반응물2-Methylthio-1,3-dithiolium perchlorateHCID 23039009—
생성물Piperazinium, 1-(1,3-dithiol-2-ylidene)-4-methyl-, perchlorateHCID 306447674.8%

반응 단계

1.2 ml of N-methylpiperazine and 1.0 g of 2-methylthio-1,3-dithiolium perchlorate were treated in the same manner as in Example 26, and the product was recrystallized from acetone-ethyl ether, whereby 0.9 g (yield: 74.8%) of 1-(1,3-dithiol-2-ylidene)-4-methylpiperazinium perchlorate (Compound No. 31) was obtained as crystals having a melting point of 192° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04737494
출처 데이터셋uspto-grants-1988_04
ORD IDord-8b72f5e7452f46b3ae8fe777be39506b
출처 메모uspto-grants-1988_04