Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → 1-[4-(4-Pyridinylamino)benzoyl]piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | 4-(4-Pyridinylamino)benzoic acid | HCID 12896000 | — |
| 생성물 | 1-[4-(4-Pyridinylamino)benzoyl]piperidine | HCID 13712474 | 49.5% |
반응 단계
1-[4-(4-Pyridinylamino)benzoyl]piperidine was prepared from 4-(4-pyridinylamino)benzoic acid and piperidine according to a procedure analogous to that of Example 48(b), and was obtained in 49.5% yield in the form of a buff powder, m.p. 170°-172° C. when recrystallized from acetonitrile.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04610991 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-64b455ccc0f942d6b583e9d13b6e7b4d |
| 출처 메모 | uspto-grants-1986_09 |